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深水 发表于 2007-3-5 19:28

150个基本的NMR实验(PDF文件)和200个NMR实验

下面列出150种基本的NMR实验名称,供有兴趣者参考.
lCgT r\;J _ (和200个NMR实验的资料见本主题帖后面的续贴)
s2o p"k Kfs 150 Basic NMR Experimentsd`#H(b(A{3a-`n
Chapter 1 The NMR Spectrometer
AmHN3T5g 1.1 Principles of an NMR Spectrometer r&P
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1.1.1 The Magnet IaRK7T
1.1.2 The Spectrometer Console MG/_(SpF[|_
1.1.3 The Workstation "l$]}#N k4n
1.1.4 Maintenance
(UV-M4vl/dq*Sd 1.2 Tuning a Probe-Head f7wi)NMS
1.2.1 Tuning and Matching with a Reflection Meter
ka?5["n*v3v-}q 1.2.2 Tuning and Matching with an R.F. Bridge and an Oscilloscope S+b_w1x
1.2.3 Tuning and Matching with a Wobble Generator
1TC__Y {t2y 1.3 The Lock Channel \2S_x2?
1.4 The Art of Shimming $M5|? EKMu
1.4.1 The Shim Gradients
0j8c-Y|#lTYV~)Si 1.4.2 The Shimming Procedure oE(Y,cL|a"Eu
1.4.3 Gradient Shimming p\.^ V8m4[
· Chapter 2 Determination of the Pulse-Duration M8mw(S~_N)B6~8@W
Exp. 2.1: Determination of the 90&; 1H Transmitter Pulse-Duration CjLe$R(P7|5g
Exp. 2.2: Determination of the 90&; 13C Transmitter Pulse-Duration
p0Hu{,a`G Exp. 2.3: Determination of the 90&; 1H Decoupler Pulse-Duration
0P
Y$IVe1V7C Exp. 2.4: The 90&; 1H Pulse with Inverse Spectrometer Configuration w#~"_aK&l)c%Qem,y2[
Exp. 2.5: The 90&; 13C Decoupler Pulse with Inverse Configuration )BAf+VQC-Q
Exp. 2.6: Composite Pulses "H| A%TI?Zm
Exp. 2.7: Radiation Damping Kq8N#ov,v
Exp. 2.8: Pulse and Receiver Phases [0P4AH(fo
Exp. 2.9: Determination of Radio Frequency Power 3]zz"AEc],F
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· Chapter 3 Routine NMR Spectroscopy and Standard Tests
:m[x!FBCX [ Exp. 3.1: The Standard 1H NMR Experiment 1?A Vuj"O3t~ M:A
Exp. 3.2: The Standard 13C NMR Experiment
"Fd
M5YXpol} Exp. 3.3: The Application of Window Functions {C`!\"[gG'j2|-V
Exp. 3.4: Computer-aided Spectral Analysis
8l$eUp ]^-^?G l Exp. 3.5: Line-Shape Test for 1H NMR Spectroscopy
RU2m7H5E(g\4C Exp. 3.6: Resolution Test for 1H NMR Spectroscopy
WFX%t/U*Qq Exp. 3.7: Sensitivity Test for 1H NMR Spectroscopy
S2}"BmVU Exp. 3.8: Line-Shape Test for 13C NMR Spectroscopy
0d:q~%_l+v P Exp. 3.9 ASTM Sensitivity Test for 13C NMR Spectroscopy
-PL}[Z1s4F1V#k Exp. 3.10: Sensitivity Test for 13C NMR Spectroscopy Q df
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Exp. 3.11: Quadrature Image Test
O7v5yo\` Exp. 3.12: Dynamic Range Test for Signal Amplitudes
(ASL"wk~ Exp. 3.13: 13&; Phase Stability Test
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NYa8pLh9m · Chapter 4 Decoupling Techniques
H*zD"o+Ec'W8P't-vB Exp. 4.1: Decoupler Calibration for Homonuclear Decoupling
?N7s)b;l){r Exp. 4.2: Decoupler Calibration for Heteronuclear Decoupling /\'[],rIU7Mc#S
Exp. 4.3: Low Power Calibration for Heteronuclear Decoupling G*PK/Yz|
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Exp. 4.4: Homonuclear Decoupling
R-DG YQ(nLqZm Exp. 4.5: Homonuclear Decoupling at Two Frequencies \uR V t;zrZ Z6N
Exp. 4.6: The Homonuclear SPT Experiment
_
? s"] nE @'t iA4rH Exp. 4.7: The Heteronuclear SPT Experiment
d.UX*kG a Exp. 4.8: 1D Nuclear Overhauser Difference Spectroscopy uHW7D7oN&gF?s
Exp. 4.9: 1D NOE Spectroscopy with Multiple Selective Irradiation ey)P DK
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Exp. 4.10: 1H Off-Resonance Decoupled 13C NMR Spectra ,k}x
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Exp. 4.11: The Gated 1H-Decoupling Technique ?&M/X?{r?2e
Exp. 4.12: The Inverse Gated 1H-Decoupling Technique
ZsvS^)RB*u/f Exp. 4.13: 1H Single Frequency Decoupling of 13C NMR Spectra .Bk-s9\NQ
Exp. 4.14: 1H Low-Power Decoupling of 13C NMR Spectra
9L.a3k-A!T Exp. 4.15: Measurement of the Heteronuclear Overhauser Effect
$gY,cN+~[4o [table=97%][tr][td]Chapter 5 Dynamic NMR Spectroscopy
xO&t-{(k+c0f1Z*FG Exp. 5.1: Low Temperature Calibration with Methanol
3iZ%PJFpL(VeK
A$L Exp. 5.2: High Temperature Calibration with 1,2-Ethanediol M2_#IP8{,\*K@+q
Exp. 5.3: Dynamic 1H NMR Spectroscopy on Dimethylformamide j0P{5Q(\5d
Exp. 5.4: The Saturation Transfer Experiment Zad)oz
Exp. 5.5: Measurement of the Rotating Frame Relaxation Time T1r p iV }q*R7XzQ
· Chapter 6 1D Multipulse Sequences
J8DqX-`.E P1b6J Exp. 6.1: Measurement of the Spin-Lattice Relaxation Time T1 1ke$l1MQ
Exp. 6.2: Measurement of the Spin-Spin Relaxation Time T2 h P(u6\ X uG+L8Cc
Exp. 6.3: 13C NMR Spectra with SEFT
6nv"jK4cT?s Exp. 6.4: 13C NMR Spectra with APT
y5XB*i%G6X;P Exp. 6.5: The Basic INEPT Technique 6j)c8Tk}*a
Exp. 6.6: INEPT+
-a'Pz0F-b!A Exp. 6.7: Refocused INEPT
!n/@Whm~ Exp. 6.8: Reverse INEPT 8KhI I&I g*g g
Exp. 6.9: DEPT-135
)vu.]{I&c[ Exp. 6.10: Editing 13C NMR Spectra with DEPT o3K@Q:id
Exp. 6.11: Multiplicity Determination with PENDANT 6P V+S3p'^3`|/P
Exp. 6.12: 1D-INADEQUATE +SsvewP{(s
Exp. 6.13: The BIRD Filter &p(a0Zkvo
Exp. 6.14: TANGO
t{)T,k.M CpZq Exp. 6.15: The Heteronuclear Double Quantum Filter !K:V/s)tZ/LJb0j
Exp. 6.16: Purging with a Spin-Lock Pulse
]/G(|R3k*N Exp. 6.17: Water Suppression by Presaturation 0T7X {:@p)^G&M4c
Exp. 6.18: Water Suppression by the Jump and Return Method nw'Z8TXF0J
· Chapter 7 NMR Spectroscopy with Selective Pulses [Z"bn8Go US+cQ
Exp. 7.1: Determination of a Shaped 90&; 1H Transmitter Pulse %WN.\3Nc3H8G-J
Exp. 7.2: Determination of a Shaped 90&; 1H Decoupler Pulse
0U|j/q%?G%YYw4@-I Exp. 7.3: Determination of a Shaped 90&; 13C Decoupler Pulse
exj7AV3i Exp. 7.4: Selective Excitation with DANTE ;]){ N]4~
Exp. 7.5: SELCOSY 8vOW9w*lfP.a
Exp. 7.6: SELINCOR: Selective Inverse H,C Correlation via 1J(C,H) Ej"b*o%E!S*`!B
Exp. 7.7: SELINQUATE
6m9I#x1e)X Exp. 7.8: Selective TOCSY 0m-d \m}_2hO
Exp. 7.9: INAPT 7]'S%_seQCG4Q3N^
Exp. 7.10: Determination of Long-Range C,H Coupling Constants
(yA&D*U(NST Exp. 7.11: SELRESOLV
9\y0`N A eV_:@ Exp. 7.12: SERF
J/k!IK?&l1o Bv!tm'Z · Chapter 8 Auxiliary Reagents, Quantitative Determinations, N(oQ@5Nnj)UA
and Reaction Mechanisms Exp. 8.1: Signal Separation Using a Lanthanide Shift Reagent %}$K!I#j"l3rH&Bg9r%~J8I
Exp. 8.2: Signal Separation of Enantiomers Using a Chiral Shift Reagent Tq5{G bc p'N4RG
Exp. 8.3: Signal Separation of Enantiomers Using a Chiral Solvating Agent Q!mxC%fb$cr"@2x
Exp. 8.4: Determination of Enantiomeric Purity with Pirkle's Reagent "gY V Nv qY
Exp. 8.5: Determination of Enantiomeric Purity by 31P NMR
+?7e f/}V Exp. 8.6: Determination of Absolute Configuration by the Advanced Mosher Method
"k?.J|9rv Y&hJ Exp. 8.7: Aromatic Solvent-Induced Shift (ASIS) sD t(ko6~aI$?y
Exp. 8.8: NMR Spectroscopy of OH-Protons and H/D Exchange rn A}sRMO
Exp. 8.9: Isotope Effects on Chemical Shielding .pJi_kJ V|
Exp. 8.10: pKa Determination with 13C NMR O\$Tl%I6}+B`Yg
Exp. 8.11: The Relaxation Reagent Cr(acac)3 fu.zn(|6W
Exp. 8.12: Determination of Paramagnetic Susceptibility by NMR ;?h"C6aT7I.ff
^
Exp. 8.13: 1H and 13C NMR of Paramagnetic Compounds
P pu'sHi{ Exp. 8.14: The CIDNP Effect 0P{z7b7r)|2qU| V
Exp. 8.15: Quantitative 1H NMR Spectroscopy: / Determination of the Alcohol Content of Polish Vodka *u(y(^U"BI*b`h
Exp. 8.16: Quantitative 13C NMR Spectroscopy with Inverse Gated 1H-Decoupling k6o0Tx7c-}L#O3P
Exp. 8.17: NMR Using Liquid-Crystal Solvents
j3X I8rsg"di)e;HY bY"@'H`Y:^
[/td][/tr][/table][color=red]还有很多，不一一列举了[/color]

lang0248cn 发表于 2007-7-6 10:55

好东西，就是不能下

lang0248cn 发表于 2007-7-6 10:56

能下了，呵呵，真好

celancelan 发表于 2007-7-6 15:28

管理员转贴贴子应该注明出处。这是我的贴子，原地址：
5`8z zQS? [url]http://www.instrument.com.cn/bbs/shtml/20050502/158325/[/url]

88dsz 发表于 2007-7-25 15:49

好东西

jackxun 发表于 2007-7-25 20:43

kan kan  xie xie  !

ccsbb 发表于 2007-8-6 00:03

dddddddd

zhangyu506 发表于 2007-10-31 13:18

太需要拉，感谢

ichyuer 发表于 2008-4-9 11:37

下了，好好研究研究~ wCJ0Rj4Z-Hp'C
最近要做好多NMR

helaojiu 发表于 2008-8-20 12:43

谢谢分享!

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